Analytical Chemistry Associated with the Destruction of Chemical Weapons

Analytical Chemistry Associated with the Destruction of Chemical Weapons

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One of the major problems associated with the disposal of chemical weapons is that the agents have degraded over time, some quite seriously. Detecting and identifying the products of this decomposition are necessary prerequisites to the safe, complete and environmentally benign destruction of stockpiled weapons. The book presents and discusses both basic and novel techniques in a variety of areas of analytical chemistry which are relevant to achieving the ultimate destruction of chemical weapons. Presentations address sample collection and preparation, mass spectrometry, chromatographic techniques, NMR, and air monitoring techniques. The work shows that analytical methods do exist to effectively support the destruction of chemical munitions. While further research is needed, the book provides an excellent baseline for further advances in the field.GC/MS Investigation of Ethyl S-2-diisopropyl Aminoethyl Methylphosphonothiolate (VX) Age Decomposition Products M. ... Capillary column GC-MS analyses were performed with GC/MS system consisting of Varian 3400 GC and Finnigan MAT ... The mass range for: EI (40-390), isobutane - CI (80-450). Before collecting of mass spectra the instrument was calibrated using FC-43 compound (perfluorotributyl amine) and CI-autotuning was performed according to the operation manual.

Title:Analytical Chemistry Associated with the Destruction of Chemical Weapons
Author: M. Heyl, Raymond R. McGuire
Publisher:Springer Science & Business Media - 2012-12-06

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